luyben11年新作PRINCIPLES AND CASE STUDIES OF SIMULTA ...?
william luyben大神的11年新作,贴个目录吧,给好评啊,亲 CONTENTS PREFACE xv 1 INTRODUCTION 1 1.1 Overview / 1 1.2 History / 3 1.3 Books / 4 1.4 Tools / 4 Reference Textbooks / 5 2 PRINCIPLES OF REACTOR DESIGN AND CONTROL 7 2.1 Background / 7 2.2 Principles Derived from Chemistry / 8 2.2.1 Heat of Reaction / 8 2.2.2 Reversible and Irreversible Reactions / 9 2.2.3 Multiple Reactions / 10 2.3 Principles Derived from Phase of Reaction / 11 2.4 Determining Kinetic Parameters / 12 2.4.1 Thermodynamic Constraints / 12 2.4.2 Kinetic Parameters from Plant Data / 13 2.5 Principles of Reactor Heat Exchange / 13 2.5.1 Continuous Stirred-Tank Reactors / 132.5.2 Tubular Reactors / 14 2.5.3 Feed-Effluent Heat Exchangers / 16 2.6 Heuristic Design of Reactor/Separation Processes / 17 2.6.1 Introduction / 17 2.6.2 Process Studied / 18 2.6.3 Economic Optimization / 21 2.6.4 Other Cases / 22 2.6.5 Real Example / 27 2.7 Conclusion / 28 References / 29 3 PRINCIPLES OF DISTILLATION DESIGN AND CONTROL 31 3.1 Principles of Economic Distillation Design / 32 3.1.1 Operating Pressure / 32 3.1.2 Heuristic Optimization / 33 3.1.3 Rigorous Optimization / 33 3.1.4 Feed Preheating and Intermediate Reboilers and Condensers / 34 3.1.5 Heat Integration / 34 3.2 Principles of Distillation Control / 35 3.2.1 Single-End Control / 36 3.2.2 Dual-End Control / 38 3.2.3 Alternative Control Structures / 38 3.3 Conclusion / 39 References / 39 4 PRINCIPLES OF PLANTWIDE CONTROL 41 4.1 History / 42 4.2 Effects of Recycle / 42 4.2.1 Time Constants of Integrated Plant with Recycle / 42 4.2.2 Recycle Snowball Effect / 43 4.3 Management of Fresh Feed Streams / 45 4.3.1 Fundamentals / 45 4.3.2 Process with Two Recycles and Two Fresh Feeds / 46 4.4 Conclusion / 52 5 ECONOMIC BASIS 53 5.1 Level of Accuracy / 53 5.2 Sizing Equipment / 54 5.2.1 Vessels / 54 5.2.2 Heat Exchangers / 555.2.3 Compressors / 56 5.2.4 Pumps, Valves, and Piping / 56 5.3 Equipment Capital Cost / 56 5.3.1 Vessels / 56 5.3.2 Heat Exchangers / 56 5.3.3 Compressors / 57 5.4 Energy Costs / 57 5.5 Chemical Costs / 57 References / 57 6 DESIGN AND CONTROL OF THE ACETONE PROCESS VIA DEHYDROGENATION OF ISOPROPANOL 59 6.1 Process Description / 60 6.1.1 Reaction Kinetics / 61 6.1.2 Phase Equilibrium / 62 6.2 Turton Flowsheet / 62 6.2.1 Vaporizer / 63 6.2.2 Reactor / 64 6.2.3 Heat Exchangers, Flash Tank, and Absorber / 64 6.2.4 Acetone Column C1 / 66 6.2.5 Water Column C2 / 66 6.3 Revised Flowsheet / 66 6.3.1 Effect of Absorber Pressure / 66 6.3.2 Effect of Water Solvent and Absorber Stages / 68 6.3.3 Effect of Reactor Size / 68 6.3.4 Optimum Distillation Design / 69 6.4 Economic Comparison / 69 6.5 Plantwide Control / 71 6.5.1 Control Structure / 71 6.5.2 Column Control Structure Selection / 75 6.5.3 Dynamic Performance Results / 76 6.6 Conclusion / 81 References / 81 7 DESIGN AND CONTROL OF AN AUTO-REFRIGERATED ALKYLATION PROCESS 83 7.1 Introduction / 84 7.2 Process Description / 84 7.2.1 Reaction Kinetics / 85 7.2.2 Phase Equilibrium / 857.2.3 Flowsheet / 86 7.2.4 Design Optimization Variables / 88 7.3 Design of Distillation Columns / 89 7.3.1 Depropanizer / 89 7.3.2 Deisobutanizer / 89 7.4 Economic Optimization of Entire Process / 91 7.4.1 Flowsheet Convergence / 91 7.4.2 Yield / 91 7.4.3 Effect of Reactor Size / 91 7.4.4 Optimum Economic Design / 93 7.5 Alternative Flowsheet / 94 7.6 Plantwide Control / 96 7.6.1 Control Structure / 96 7.6.2 Controller Tuning / 100 7.6.3 Dynamic Performance / 101 7.7 Conclusion / 103 References / 105 8 DESIGN AND CONTROL OF THE BUTYL ACETATE PROCESS 107 8.1 Introduction / 108 8.2 Chemical Kinetics and Phase Equilibrium / 108 8.2.1 Chemical Kinetics and Chemical Equilibrium / 108 8.2.2 Vapor-Liquid Equilibrium / 110 8.3 Process Flowsheet / 112 8.3.1 Reactor / 112 8.3.2 Column C1 / 113 8.3.3 Column C2 / 113 8.3.4 Column C3 / 113 8.3.5 Flowsheet Convergence / 115 8.4 Economic Optimum Design / 117 8.4.1 Reactor Size and Temperature / 117 8.4.2 Butanol Recycle and Composition / 118 8.4.3 Distillation Column Design / 119 8.4.4 System Economics / 120 8.5 Plantwide Control / 121 8.5.1 Column C1 / 121 8.5.2 Column C2 / 122 8.5.3 Column C3 / 1228.5.4 Plantwide Control Structure / 123 8.5.5 Dynamic Performance / 124 8.6 Conclusion / 133 References / 133 9 DESIGN AND CONTROL OF THE CUMENE PROCESS 135 9.1 Introduction / 136 9.2 Process Studied / 136 9.2.1 Reaction Kinetics / 136 9.2.2 Phase Equilibrium / 137 9.2.3 Flowsheet / 137 9.3 Economic Optimization / 140 9.3.1 Increasing Propylene Conversion / 140 9.3.2 Effects of Design Optimization Variables / 141 9.3.3 Economic Basis / 142 9.3.4 Economic Optimization Results / 143 9.4 Plantwide Control / 147 9.5 Conclusion / 158 References / 158 10 DESIGN AND CONTROL OF THE ETHYL BENZENE PROCESS 159 10.1 Introduction / 159 10.2 Process Studied / 160 10.2.1 Reaction Kinetics / 161 10.2.2 Phase Equilibrium / 162 10.2.3 Flowsheet / 163 10.3 Design of Distillation Columns / 164 10.3.1 Column Pressure Selection / 166 10.3.2 Number of Column Trays / 169 10.4 Economic Optimization of Entire Process / 169 10.5 Plantwide Control / 172 10.5.1 Distillation Column Control Structure / 172 10.5.2 Plantwide Control Structure / 173 10.5.3 Controller Tuning / 174 10.5.4 Dynamic Performance / 174 10.5.5 Modified Control Structure / 176 10.6 Conclusion / 183 References / 18311 DESIGN AND CONTROL OF A METHANOL REACTOR/COLUMN PROCESS 185 11.1 Introduction / 185 11.2 Process Studied / 186 11.2.1 Compression and Reactor Preheating / 186 11.2.2 Reactor / 187 11.2.3 Separator, Recycle, and Vent / 187 11.2.4 Flash and Distillation / 188 11.3 Reaction Kinetics / 188 11.4 Overall and Per-Pass Conversion / 189 11.5 Phase Equilibrium / 191 11.6 Effects of Design Optimization Variables / 192 11.6.1 Economic Basis / 192 11.6.2 Effect of Pressure / 193 11.6.3 Effect of Reactor Size / 195 11.6.4 Effect of Vent/Recycle Split / 196 11.6.5 Effect of Flash-Tank Pressure / 197 11.6.6 Optimum Distillation Column Design / 198 11.7 Plantwide Control / 201 11.7.1 Control Structure / 201 11.7.2 Column Control Structure Selection / 203 11.7.3 High-Pressure Override Controller / 203 11.7.4 Dynamic Performance Results / 204 11.8 Conclusion / 209 References / 210 12 DESIGN AND CONTROL OF THE METHOXY-METHYL-HEPTANE PROCESS 211 12.1 Introduction / 211 12.2 Process Studied / 212 12.2.1 Reactor / 212 12.2.2 Column C1 / 213 12.2.3 Column C2 / 213 12.2.4 Column C3 / 213 12.3 Reaction Kinetics / 213 12.4 Phase Equilibrium / 215 12.5 Design Optimization / 215 12.5.1 Economic Basis / 216 12.5.2 Reactor Size versus Recycle Trade-Off / 21612.6 Optimum Distillation Column Design / 220 12.6.1 Column Pressures / 220 12.6.2 Number of Stages / 220 12.6.3 Column Profiles / 222 12.7 Plantwide Control / 223 12.7.1 Control Structure / 225 12.7.2 Dynamic Performance Results / 227 12.8 Conclusion / 230 References / 231 13 DESIGN AND CONTROL OF A METHYL ACETATE PROCESS USING CARBONYLATION OF DIMETHYL ETHER 233 13.1 Introduction / 233 13.2 Dehydration Section / 234 13.2.1 Process Description of Dehydration Section / 234 13.2.2 Dehydration Kinetics / 235 13.2.3 Alternative Flowsheets / 236 13.2.4 Optimization of Three Flowsheets / 240 13.3 Carbonylation Section / 245 13.3.1 Process Description / 246 13.3.2 Carbonylation Kinetics / 247 13.3.3 Effect of Parameters / 248 13.3.4 Flowsheet Convergence / 250 13.3.5 Optimization / 251 13.4 Plantwide Control / 255 13.4.1 Control Structure / 255 13.4.2 Dynamic Performance / 261 13.5 Conclusion / 262 References / 262 14 DESIGN AND CONTROL OF THE MONO-ISOPROPYL AMINE PROCESS 263 14.1 Introduction / 263 14.2 Process Studied / 264 14.2.1 Reaction Kinetics / 264 14.2.2 Phase Equilibrium / 265 14.2.3 Flowsheet / 266 14.3 Economic Optimization / 268 14.3.1 Design Optimization Variables / 268 14.3.2 Optimization Results / 26914.4 Plantwide Control / 270 14.4.1 Dynamic Model Sizing / 271 14.4.2 Distillation Column Control Structures / 272 14.4.3 Plantwide Control Structure / 276 14.5 Conclusion / 289 References / 290 15 DESIGN AND CONTROL OF THE STYRENE PROCESS 291 15.1 Introduction / 292 15.2 Kinetics and Phase Equilibrium / 293 15.2.1 Reaction Kinetics / 293 15.2.2 Phase Equilibrium / 294 15.3 Vasudevan et al. Flowsheet / 295 15.3.1 Reactors / 295 15.3.2 Condenser and Decanter / 295 15.3.3 Product Column C1 / 296 15.3.4 Recycle Column C2 / 298 15.4 Effects of Design Optimization Variables / 298 15.4.1 Effect of Process Steam / 298 15.4.2 Effect of Reactor Inlet Temperature / 301 15.4.3 Effect of Reactor Size / 302 15.4.4 Optimum Distillation Column Design / 303 15.4.5 Number of Reactors / 304 15.4.6 Reoptimization / 304 15.4.7 Other Improvements / 305 15.5 Proposed Design / 305 15.6 Plantwide Control / 306 15.6.1 Control Structure / 306 15.6.2 Column Control Structure Selection / 310 15.6.3 Dynamic Performance Results / 312 15.7 Conclusion / 317 References / 317 NOMENCLATURE 319 INDEX 321
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9人参与回答
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luyben大师的好东东,珍贵资源,谢谢分享!!
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luyben的东西一向都很给力,先下了再说。。。
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谢谢楼主分享luben大师的资料!书中有许多化工工艺过程与控制的的实例。
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luyben的书,好好看看。 谢谢楼主分享了!!!!
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好东西!真是不错的东西!谢谢楼主分享!下载学习学习!
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下载看看有什么新的内容. 有例子文件么????
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学习一下
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真是不错,有时间多去交流一下,指导指导我们菜鸟 我没有发布群号,是系统加上去的
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赞,在wiley鼓捣半天没能弄下来