请教：关于TBSCL保护基问题？ tbs保护酚羟基没有问题的 可参考以下 to a solution of 5 (50 mg, 0.14 mmol) and iminazole (9 mg, 0.14 mmol) in dcm (3ml) cooled to 0℃ was added tbscl (21 mg, 0.14 mmol). the resulting mixture was stirred at rt for 10 min. the reaction mixture was washed with water and concentrated to give the crude product. the crude product was purified by prepare tlc to give the desired product.查看更多
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