求帮忙翻译下，重氮化方面的？ example 3 例３ benzene diazonium fluoride was prepared substantially in accordance with the procedure of example 1 except that the temperature of the refrigerated bath of glycol and water was maintained at plus 5.degree. c. 除了乙二醇与水的冷冻温度维持在５℃以上，氯苯重盐的配制的大体在采用例一的程序。 the temperature of the reaction mixture exiting each static mixer in the first four sections was higher (35.degree. c., maximum temperature in each such section). the temperature of the reaction mixture exiting each static mixer in the last six sections was also higher (about 20.degree. c., maximum temperature in each such section). 第一级４段各静混合器中反应混合物的温度更高（每一段最高温度达３５℃）。最后６段反应中各反应混合物温度也更高（每一段最高温度约达２０℃）。 the resulting mixture exiting the cross-flow tubular reactor was a dark brownish-black solution. analysis of the samples of the exiting stream showed presence of benzene diazonium fluoride in lower concentrations of from about 2.05 to about 2.17 g-moles per liter, corresponding to a diazonium fluoride yield of about 85 to 90% based on the amount of nitrosyl fluoride introduced into the reactor. 错流管式反应器合成混合物是深棕黑色反应物。下游取样分析显示出低浓度的氯苯重盐，含量约为2.05至2.17克分子/升，相当于引入反应器亚硝酰氟达到85至90%氯重盐产量。 个人理解，请专业人士指点，谢谢！！查看更多
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