这个怎么成球的,真心没搞懂,请教各位呀~?吹狡南? 是用[C4mim]Cl 这种离子液体溶解纤维素的,这怎么成bead的呢?A solution of approximately 10 wt %microcrystalline cellulose (4.8 g) in [C4mim]Cl (50.0 g) wasprepared using microwave pulse heating.9 The solution wascooled to 60 °C, and 1.0 g of bovine serum albumin (BSA)was added and homogenized to prepare a mixture containing1:5 wt % ratio of BSA:cellulose. The material was formedinto beads by dispersing the solution in a rapidly stirringhot (100 °C) poly(propylene glycol) (PPG 425; Fluka, BuchsSG, Switzerland) bath using an overhead ultrahigh-torquestirrer (Caframo Limited, Wiarton, Ontario) set at 850 rpm.The [C4mim]Cl/cellulose/BSA mixture was slowly added tothe stirring, hot PPG and dispersed to form small beads.During stirring (30 min), the temperature of the PPG bathwas allowed to fall to approximately 40 °C, facilitating ahardening (reconstitution) of the outer surface of the [C4-mim]Cl/cellulose/BSA beads, preventing subsequent agglomeration.The solution was removed from the stirrer, andEtOH was slowly added to further reconstitute the beads andwash the remaining PPG from the material. The beads werewashed five times with EtOH followed by five washings withDI H2O and then filtered using a set of mesh filters,查看更多