纳米四氧化三铁负载金属镍问题?Ferrite magnetic nanoparticlesFe3O4 (2 g) and NiCl2·6H2O (10 wt% of nickel on ferrite) were stirred atroom temperature in aqueous solution for 1 h. After impregnation, thesuspension was adjusted to pH 12 by adding sodium hydroxide (0.5m)and stirred for 10 to 12 h. The solid was washed by distilled water (510 mL). The obtained metal precursors were reduced by adding an aqueoussolution of 0.2m NaBH4 dropwise under gentle stirring in an ice–water bath for 30 min until no bubbles were observed in the solution.The resulting Fe3O4Ni MNPs were ultrasonicated for 10 min and thenwashed with distilled water and subsequently with ethanol. The synthesizedFe3O4Ni MNPs were characterized by several techniques such asXRD, ICP-AES, TEM, and FEG-SEM-EDS.,请问这里面的硼氢化钠应该怎么处理?我直接配制的 硼氢化钠溶液 加到溶液中去,没有得到理想效果。查看更多7个回答 . 3人已关注