请教关于氨基与CbzCl的反应? 用英文你想看得话: to a solution of 1 eq. of amine in water contaning 1.1 eq of base(naoh or tea) was added under ice bath 1.1 eq of cbzcl, after stirring at this temperature for 10 min, it was stirred at rt for 1 hour, then the solvent was extracted with ether and the organic layer was then washed by water and brine, it was then dried over na2so4. then it was purified on column chromatograhy. 仅供参考。 查看更多