主编提了个XPS表征的质疑,不知道怎么解答?审稿人认为你把Pd归属为价态高于+2的物种是不适合的!至于怎么回答,需要看你的上下文了,载体?前处理条件?使用条件等? 主要是这句话: XPS is notorious for initial and final state effects as well as reference peak shifts that make oxidation state assignments confusing.其不是说XPS用来判断价态是不准确的吗?还有他提到的原因,我不知道是什么意思 initial and final state effects as well as reference peak shifts查看更多