如何各位如何合成这个化合物?？ 给你找了一篇文献，建议您看看。上欧洲专利就可以免费提取的，专利号是us20050027146 united states patent application 20050027146 kind code a1 martinez, rodolfo a. ; et al. february 3, 2005 synthesis of isotopically labeled r- or s-[13c, 2h] glycerols abstract the present invention is directed to asymmetric chiral labeled glycerols including at least one chiral atom, from one to two .sup.13c atoms and from zero to four deuterium atoms bonded directly to a carbon atom, e.g., (2s)[1,2-.sup.13c.sub.2]glycerol and (2r)[1,2-.sup.13c.sub.2]glycerol, and to the use of such chiral glycerols in the preparation of labeled amino acids. inventors: martinez, rodolfo a. ; (santa fe, nm) ; unkefer, clifford j. ; (los alamos, nm) ; alvarez, marc a. ; (santa fe, nm) correspondence name and address: university of california los alamos national laboratory p.o. box 1663, ms a187 los alamos nm 87545 us serial no.: 629982 series code: 10 filed: july 30, 2003 u.s. current class: 568/852 u.s. class at publication: 568/852 intern'l class: c07c 035/22; c07c 035/24 united states patent application 20050027146 kind code a1 martinez, rodolfo a. ; et al. february 3, 2005 synthesis of isotopically labeled r- or s-[13c, 2h] glycerols abstract the present invention is directed to asymmetric chiral labeled glycerols including at least one chiral atom, from one to two .sup.13c atoms and from zero to four deuterium atoms bonded directly to a carbon atom, e.g., (2s)[1,2-.sup.13c.sub.2]glycerol and (2r)[1,2-.sup.13c.sub.2]glycerol, and to the use of such chiral glycerols in the preparation of labeled amino acids. inventors: martinez, rodolfo a. ; (santa fe, nm) ; unkefer, clifford j. ; (los alamos, nm) ; alvarez, marc a. ; (santa fe, nm) correspondence name and address: university of california los alamos national laboratory p.o. box 1663, ms a187 los alamos nm 87545 us serial no.: 629982 series code: 10 filed: july 30, 2003 u.s. current class: 568/852 u.s. class at publication: 568/852 intern'l class: c07c 035/22; c07c 035/24 查看更多
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